[meteorite-list] question on performing a nickel test
From: al mitterling <almitt_at_meteoritecentral.com>
Date: Sat, 20 Dec 2008 17:55:51 -0500 Message-ID: <A66F34C0D8944FDA93AA0EAF44BB96E6_at_StarmanPC> Hi Mike and all, In Richard Norton's new field guide, he lists some house hold chemicals that you can use to preform a nickel test also. I need to look it up and let people know which page. Haven't tried it yet but I am sure that Richard Norton has. One other problem with the jewlery nickel test kits I think, is that they tend to expire. Don't know if the chemicals have useful life span or not but had trouble with one at a show I was doing to show the nickel test result. All my best. --AL Mitterling ----- Original Message ----- From: "Randy Korotev" <korotev at wustl.edu> To: <meteorite-list at meteoritecentral.com> Sent: Saturday, December 20, 2008 2:19 PM Subject: Re: [meteorite-list] question on performing a nickel test > Mike: > > I've had the same experience. The problem, I think, is that the DMG test > is actually TOO sensitive to nickel. All meteoritic metal is >5% (50,000 > ppm) Ni. Metals with only a few hundred ppm Ni will give a positive > result with DMG test, however. I think many steels and cast irons may > have a few hundred ppm Ni. > > This subject came up a few years ago on this list and someone (I forget > who) mentioned that in his experience, the swab stayed pink quite a bit > longer with a real meteorite metal while the pink faded in an hour with > "false positives." > > Randy Korotev > > > > > > > > At 14:09 19-12-08 Friday, you wrote: >>Hi List, >> >>If someone has experience with the Allerderm Nickel test and wouldn't >>mind sharing their knowledge of how to do it... >> >>I am attempting to do a nickel test at home here and I ran into a bit >>of a snag. I have a piece of iron that most likely is not a piece of >>meteoritic iron that I was using as a test piece. I sanded a surface >>on it, cleaned it with alcohol several times, got out the trusty >>Allertest NI test kit from Allerderm, placed a drop each of the >>little bottles onto a cotton swab, and placed that on the cleaned >>surface of the metal. Using this piece of iron as a control piece, I >>wanted to be sure I wasn't doing something in the steps I was using >>that would cause me to get a false positive. On this test - test, >>the swab turned pink quickly. If I do the exact steps only add in >>placing a drop of white vinegar on the cleaned surface, wait a couple >>minutes and then apply the nickel test, I get almost a blood red swab >>in just the first second. The first time I did this test and saw >>this, I thought I had contaminated the surface so I sanded it again >>down to a fresh surface, cleaned it several times again with alcohol >>before attempting the nickel test without vinegar. Second time, same >>result. When using a drop of vinegar again, same result - blood red >>quickly. >> >>What am I doing wrong, if anything? Could I still have contamination >>on the metal that the sanding and cleaning with alcohol is not removing? >> >>Mike in CO >>______________________________________________ >>http://www.meteoritecentral.com >>Meteorite-list mailing list >>Meteorite-list at meteoritecentral.com >>http://six.pairlist.net/mailman/listinfo/meteorite-list >> > > > ______________________________________________ > http://www.meteoritecentral.com > Meteorite-list mailing list > Meteorite-list at meteoritecentral.com > http://six.pairlist.net/mailman/listinfo/meteorite-list > > Received on Sat 20 Dec 2008 05:55:51 PM PST |
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