[meteorite-list] Stardust in the Laboratory

From: Ron Baalke <baalke_at_meteoritecentral.com>
Date: Mon Feb 20 23:58:18 2006
Message-ID: <200602210456.k1L4uY626799_at_zagami.jpl.nasa.gov>


Public release date: 20-Feb-2006

Contact: Susan Killenberg McGinn
Washington University in St. Louis

Stardust in the laboratory

Space science discoveries are being made in earthly labs

Reaching for the stars isn't so out of reach these days.

With the development of increasingly sophisticated instruments,
researchers not only are able to get more detailed information about
circumstellar and interstellar dust from afar by using advanced
telescopes, but they also are now able to study actual stardust right in
their own labs.

Since the discovery two decades ago that primitive meteorites contain
microscopic grains of preserved stardust, physicists, chemists,
astrophysicists and astronomers have taken advantage of this
interstellar material that falls to Earth.

With new and ever-improving instruments to analyze these grains in the
laboratory, researchers around the world are gaining new insights into
the formation of the elements and the evolution of stars.

And with the successful January 2006 completion of NASA's seven-year
2.88 billion mile round-trip Stardust mission to collect cometary and
interstellar dust particles, researchers worldwide will be busy
analyzing these samples for years to come looking for answers to
fundamental questions about comets and the origin of the solar system.

Ernst K. Zinner, Ph.D., research professor of physics and of earth and
planetary sciences, both in Arts & Sciences, at Washington University in
St. Louis, provided an overview of the study of "Stardust in the
Laboratory" Monday, Feb. 20, 2006, at the annual meeting of the American
Association for the Advancement of Science (AAAS), held in St. Louis. He
also participated in the AAAS "Exploring a Dusty Cosmos" press briefing
that morning.

Zinner, the recipient of both the National Academy of Sciences' J.
Lawrence Smith Medal and the Meteoritical Society's Leonard Medal, is a
pioneer in the analysis of stellar dust grains found in primitive

In 1987, Zinner and colleagues at Washington University and a group of
scientists at the University of Chicago found the first stardust in a
meteorite. Those presolar grains were specks of diamond and silicon

Since then, Zinner and other members of WUSTL's Laboratory for Space
Sciences' research group have played leading roles in analyzing these
grains in the laboratory and interpreting the results. The Laboratory
for Space Sciences is part of the departments of Physics and Earth and
Planetary Sciences and the McDonnell Center for the Space Sciences, all
in Arts & Sciences.

It is generally believed that these grains were formed billions of years
ago in the atmospheres of dying stars. "As a star dies," Zinner
explains, "its atmosphere begins to expand and cool. Then ions turn into
atoms, atoms form molecules and, eventually, molecules condense into

The dust then is ejected into outer space, where it collects with gas
and dust from other stars to form cold, dark clouds.

More than 4.5 billion years ago, one such cloud collapsed to form our
solar system, and the dust -- literally pieces of distant and long-dead
stars -- was preserved in meteorites.

By studying the isotopic composition of these grains, researchers are
gaining new information on nuclear and chemical processes in stars and
on conditions during the formation of the solar system.

Advancements in instrumentation

Using a microanalytic instrument called an ion microprobe to measure the
proportions of specific isotopes, Zinner and his colleagues in the late
1980s and '90s identified three types of interstellar grains -- silicon
carbide, graphite and aluminum oxide -- and two important stellar
sources of the grains.

The researchers determined through signature isotopic compositions that
the grains came from red giant stars of low to medium mass during late
stages of their evolution and from supernovae, massive stars that
exploded at the end of their evolution.

These grains, Zinner explains, condensed when the envelope of red giants
cooled during expansion or when supernovae exploded, thus preserving the
elemental and isotopic composition of their stellar sources.

Zinner adapted the microprobe to permit precise isotopic measurements in
samples weighing as little as a millionth of a millionth of a gram.

Isotopes are versions of an element that have different numbers of
neutrons and, consequently, different masses. In the same way that a
zoologist studies a set of footprints to learn about the animal that
made them, Zinner and his colleagues study the isotopes in a grain to
learn about the parent star -- its mass, age, composition and other

The latest ion microprobe on the scene is the NanoSIMS (SIMS is short
for Secondary Ion Mass Spectrometer), which can resolve objects smaller
than a micrometer -- one millionth of a meter -- or 1/100th smaller than
the diameter of a human hair.

Zinner and Frank J. Stadermann, Ph.D., senior research scientist in the
Department of Physics in Arts & Sciences, helped design and test the
NanoSIMS, which is made by CAMECA in Paris. At a cost of $2 million,
Washington University acquired the first NanoSIMS in the world in 2000.
There are now some 16 worldwide.

Ion probes direct a beam of ions onto one spot on a sample. The beam
dislodges some of the sample's own atoms, some of which become ionized.
This secondary beam of ions enters a mass spectrometer that is set to
detect a particular isotope. Thus, ion probes can identify grains that
have an unusually high or low proportion of that isotope.

Unlike most other ion probes, however, the NanoSIMS can detect five
different isotopes simultaneously. The beam can also travel
automatically from spot to spot so that many hundreds or thousands of
grains can be analyzed in one experimental setup.

Using the NanoSIMS, Ann Nguyen, Ph.D., at the time a WUSTL graduate
student under Zinner, persevered -- after a WUSTL team had already
sifted through 100,000 grains looking for a particular type of stardust
without success -- and found the first silicate stardust in a meteorite.

In the March 5, 2004, issue of Science, Nguyen and Zinner describe nine
specks of silicate stardust -- presolar silicate grains -- from one of
the most primitive meteorites known. Silicate is a compound of silicon,
oxygen and other elements such as magnesium and iron. Nguyen is now a
postdoctoral research associate in the Department of Terrestrial
Magnetism at the Carnegie Institution in Washington, D.C.

"Finding presolar silicates in a meteorite tells us that the solar
system formed from gas and dust, some of which never got very hot,
rather than from a hot solar nebula," Zinner says. "Analyzing such
grains provides information about their stellar sources, nuclear
processes in stars and the physical and chemical compositions of stellar

"The NanoSIMS was essential for this discovery," Zinner says. "These
presolar silicate grains are very small -- only a fraction of a
micrometer. The instrument's high spatial resolution and high
sensitivity made these measurements possible."

This detailed information about stardust proves that space science can
be done in the laboratory, Zinner says. "Analyzing these small specks
can give us information, such as detailed isotopic ratios, that cannot
be obtained by the traditional techniques of astronomy," he adds.

Other instrumentation being used for studying very small particles
include various kinds of mass spectrometers for chemical and isotopic
analysis and radioactive dating, electron microscopes for chemical and
structural analysis, and chemical and physical apparatus geared to the
processing of microscopic material.

Zinner and Stadermann's current project will be analyzing the three
slices of a cometary dust particle they recently received from the
Stardust mission -- the first U.S. mission since Apollo 17 in 1972 to
bring back extraterrestrial material.


WUSTL's Laboratory for Space Sciences' research group has a long
tradition of analyzing such material up close and personal. WUSTL
researchers were some of the first to receive lunar samples brought to
Earth from both the Apollo 11 mission in 1969 and from Apollo 17.

Received on Mon 20 Feb 2006 11:56:34 PM PST

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