[meteorite-list] Simplified Meteorite Rust treatment
From: David Hardy <mdavidhardy_at_meteoritecentral.com>
Date: Thu Apr 22 09:46:21 2004 Message-ID: <20010501174636.3682.qmail_at_web13804.mail.yahoo.com> Hi Steve, Will this work on uncut irons? David --- meteorites_at_space.com wrote: > Over the years I have been experimenting with various methods of neutralizing > FeCl3 and NiCl3 (Cl2 also) in meteorites. > > Now I have found that it can be done with 70% isopropyl rubbing alcohol right > off the drug store shelf, and Red Devil lye (sodium hydroxide). > > Use as much isopropyl to cover the specimen in a glass or tupperware > container, then add a teaspoon of Red Devil lye, or as much as the solution > can absorb. If after a few days the first teaspoon dissolves, then add a bit > more. This can be done with or without the specimen in the solution. > > Let the specimen soak in the container (covered) for a week or more. Don't > be alarmed to see rusticles (sort of like those on the Titanic) forming. > This is a clear indication that the chemical reaction is taking place, and > the Cl is being absorbed by the Na in the solution, and the OH is attaching > in its stead to the Fe forming a non corrosive FeOH and or NiOH. (These are > the "rusticles" that you see) > > If during this time you see that the solution is turning rust brown, pour it > and add fresh 70% isoproypl and another dash of Red Devil lye. After a week > or two. Remove the specimen from the solution and allow it to dry. After a > few days lightly sand it to remove the rusticles, then set it uncoated for a > week or more to see if it still bleeds chlorides of iron or nickel. If it > does, repeat the process for another week or more. > I have found this process to work well with Mt. Dieu, Brahin, Brenham, Canyon > Diablo, Campo del Cielo, and other rusters. With pallasites, the crystals > will sometimes rise a bit in their sockets, but once dry the FeOH that holds > them will turn into tougher iron oxides. Sanding it down will make the > surface level again. And I have found that after the light sanding, a day or > so additional soak of pallasites is a good idea. Then dry and polish > afterwards. For the really stubborn specimens, I will be working on a simple > electrolosis addition to the above mentionned solution. This involves using > a battery and a good resistor to create a small current that will drive the > Cl ions out of and away from the meteorite. Will post as soon as I test the > idea and get some solid results. Steve Schoner, American Meteorite Survey; > http://www.geocities.com/american_meteorite_survey > > ___________________________________________________________________ > Join the Space Program: Get FREE E-mail at http://www.space.com. > > _______________________________________________ > Meteorite-list mailing list > Meteorite-list_at_meteoritecentral.com > http://www.pairlist.net/mailman/listinfo/meteorite-list __________________________________________________ Do You Yahoo!? Yahoo! Auctions - buy the things you want at great prices http://auctions.yahoo.com/ Received on Tue 01 May 2001 01:46:36 PM PDT |
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